Webb2 atmosphere, protocatechualdehyde (41.4 g, 0.30 mol) was dissolved in 350 mL of ethanol. Then, 4,40-diaminodiphenyl ether (19.8 g, 0.10 mol) was slowly added into this system. A er continuous stirring for 30 min at room temperature, the system was heated to 80 C and stirred for 6 h. A erward, the mixture was cooled down and transferred to ice ... WebbThe hydroxide solution is washed with ether and then acidified with dilute sulfuric acid. The acidic solution is extracted with ether, dried, and then distilled off to leave 12.8 g of protocatechualdehyde. Methylenate this with the procedure listed in the safrole section replacing the 4-allyl catechol with 138 g of protocatechualdehyde.
Protocatechualdehyde - an overview ScienceDirect Topics
Webb3,4-Dihydroxybenzaldehyde (Protocatechualdehyde) may be employed as starting reagent for the synthesis of 4-vinylbenzocrown ether. 3,4-Dihydroxybenzaldehyde may be used for the surface modification of nanocrystalline TiO 2 particles. WebbCategory: flavoring agents. Recommendation for 3,4-dihydroxybenzaldehyde usage levels up to: not for fragrance use. Maximised Survey-derived Daily Intakes (MSDI-EU): 8.50 (μg/capita/day) Modified Theoretical Added Maximum Daily Intake (mTAMDI): 1600 (μg/person/day) Threshold of Concern: blackish good dre hunting
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WebbDescription. Protocatechuic aldehyde is a polyphenol found in many plants and foods; it exhibits anti-inflammatory, cardioprotective, anti-atherosclerotic, and hepatoprotective … Webb8 apr. 2003 · 138g protocatechualdehyde 120 ml 50% NaOH aqueous solution (91g NaOH, 91g dH2O) 500 ml dimethylsulfoxide (DMSO) 120ml (160g) dichloromethane (DCM). … WebbA process for preparing protocatechualdehyde or a 3-alkoxy-4-hydroxybenzaldehyde which comprises subjecting catechol or a 2-alkoxyphenol to reaction with glyoxylic acid in a basic aqueous medium in the presence of a catalyst containing one or more compounds selected from aluminium oxide, silicon oxide and hydrated aluminium oxide in an … ganache chocolat au lait thermomix